2OBZ
Crystal structure of the The brominated Z-DNA duplex d(CGCG[BrU]G)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-ID |
| Synchrotron site | APS |
| Beamline | 19-ID |
| Temperature [K] | 100 |
| Collection date | 2000-03-01 |
| Wavelength(s) | 0.9199 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 17.339, 32.074, 44.341 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 25.980 - 1.100 |
| R-factor | 0.20227 |
| Rwork | 0.202 |
| R-free | 0.21332 |
| Structure solution method | SAD |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.686 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | SHARP |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 26.000 | |
| High resolution limit [Å] | 1.100 | 1.100 |
| Number of reflections | 9673 | |
| Completeness [%] | 96.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
