2NXV
Structure of the 6th ORF of the Rhodobacter blastica ATPase operon; Majastridin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I911-3 |
Synchrotron site | MAX II |
Beamline | I911-3 |
Detector technology | CCD |
Detector | MAR CCD 165 mm |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 121.873, 90.311, 69.590 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.960 - 1.100 |
R-factor | 0.13809 |
Rwork | 0.137 |
R-free | 0.15544 |
Structure solution method | SAD based on native sulphurs |
RMSD bond length | 0.016 |
RMSD bond angle | 1.638 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHELXS |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 72.560 | 1.160 |
High resolution limit [Å] | 1.100 | 1.100 |
Rmerge | 0.050 | 0.355 |
Number of reflections | 295175 | |
<I/σ(I)> | 7.8 | 2.2 |
Completeness [%] | 95.3 | 71.2 |
Redundancy | 4.4 | 2.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |