2NTT
Crystal Structure of SEK
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE F2 |
| Synchrotron site | CHESS |
| Beamline | F2 |
| Detector technology | AREA DETECTOR |
| Wavelength(s) | 0.9779 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 53.774, 45.790, 90.696 |
| Unit cell angles | 90.00, 90.02, 90.00 |
Refinement procedure
| Resolution | 34.670 - 1.561 |
| R-factor | 0.165 |
| Rwork | 0.163 |
| R-free | 0.20200 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | SpeI |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.229 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | AMoRE |
| Refinement software | REFMAC (5.2) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 34.670 | |
| High resolution limit [Å] | 1.561 | 1.561 |
| Number of reflections | 63074 | |
| <I/σ(I)> | 30.9 | |
| Redundancy | 3.6 | 2.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | VAPOR DIFFUSION, HANGING DROP |
