Experimental procedure
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 60.832, 38.293, 42.211 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.000 - 2.000 |
| R-factor | 0.198 |
| RMSD bond length | 0.026 |
| RMSD bond angle | 0.046 |
| Refinement software | PROFFT |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 2.400 * |
| High resolution limit [Å] | 2.000 * |
| Rmerge | 0.080 * |
| Total number of observations | 5758 * |
| Number of reflections | 2705 * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 7.2 * | Anderson, D., (1980) J.Biol.Chem., 255, 2578. * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | 10-20 (mg/ml) | ||
| 2 | 1 | drop | 5 (M) | ||
| 3 | 1 | drop | ammonium sulfate | 5 (Msat) | pH7.2 |
| 4 | 1 | drop | sodium phosphate | 0.02 (M) | pH7.2 |
| 5 | 1 | reservoir | 5 (M) | ||
| 6 | 1 | reservoir | sodium phosphate | 0.02 (M) | pH7.2 |
