2LGS

FEEDBACK INHIBITION OF FULLY UNADENYLYLATED GLUTAMINE SYNTHETASE FROM SALMONELLA TYPHIMURIUM BY GLYCINE, ALANINE, AND SERINE

Experimental procedure

Spacegroup name	C 1 2 1
Unit cell lengths	235.500, 134.500, 200.100
Unit cell angles	90.00, 102.80, 90.00

Refinement procedure

Resolution	8.000 - 2.800
R-factor	0.235
Rwork	0.235
RMSD bond length	0.011
RMSD bond angle	3.002
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.800 *
Rmerge	0.060 *
Total number of observations	170218 *
Number of reflections	110184 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	peptide	2 (mg/ml)
2	1	reservoir	potassium phosphate-sodium hydroxide	0.05 (M)
3	1	reservoir	ammonium sulfate	2.95 (M)