2JLU
Dengue virus 4 NS3 helicase in complex with ssRNA
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 100 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 132.033, 105.497, 72.517 |
| Unit cell angles | 90.00, 117.54, 90.00 |
Refinement procedure
| Resolution | 20.000 - 2.040 |
| R-factor | 0.19935 |
| Rwork | 0.197 |
| R-free | 0.24198 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2jlq |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.329 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.800 | 2.100 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.090 | 0.380 |
| Number of reflections | 54798 | |
| <I/σ(I)> | 17.4 | 4.2 |
| Completeness [%] | 96.5 | 86.4 |
| Redundancy | 6.4 | 6.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
