2JIE
BETA-GLUCOSIDASE B FROM BACILLUS POLYMYXA COMPLEXED WITH 2-F-GLUCOSE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM16 |
Synchrotron site | ESRF |
Beamline | BM16 |
Temperature [K] | 120 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 71.236, 74.647, 88.754 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.000 - 2.300 |
R-factor | 0.2498 |
Rwork | 0.250 |
R-free | 0.30610 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1e4i |
RMSD bond length | 0.010 |
RMSD bond angle | 1.638 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 2.320 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.090 | 0.380 |
Number of reflections | 24641 | |
<I/σ(I)> | 16 | 3.4 |
Completeness [%] | 99.8 | 100 |
Redundancy | 10.4 | 10.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |