2JHQ
Crystal structure of Uracil DNA-glycosylase from Vibrio cholerae
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-01-12 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 60.140, 60.440, 61.330 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.310 - 1.500 |
R-factor | 0.177 |
Rwork | 0.175 |
R-free | 0.21000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1eug |
RMSD bond length | 0.011 |
RMSD bond angle | 1.329 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 12.000 | 1.580 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.080 | 0.480 |
Number of reflections | 36324 | |
<I/σ(I)> | 12.5 | 2.9 |
Completeness [%] | 99.7 | 100 |
Redundancy | 3.9 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | 50 MM MES AT PH 6.0. 28% (W/V) POLYETHYLENE GLYCOL (PEG) 3350. |