2JH2
X-ray crystal structure of a cohesin-like module from Clostridium perfringens
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 113 |
Spacegroup name | H 3 2 |
Unit cell lengths | 106.776, 106.776, 221.309 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 2.500 |
R-factor | 0.235 |
Rwork | 0.232 |
R-free | 0.29500 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.077 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | PHASER |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.590 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.070 | 0.420 |
Number of reflections | 16275 | |
<I/σ(I)> | 13.6 | 3.9 |
Completeness [%] | 99.9 | 99 |
Redundancy | 6.2 | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |