2JG2
HIGH RESOLUTION STRUCTURE OF SPT WITH PLP INTERNAL ALDIMINE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-10-09 |
Detector | MARRESEARCH |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 74.190, 107.552, 90.322 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 18.790 - 1.300 |
R-factor | 0.155 |
Rwork | 0.153 |
R-free | 0.18500 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.020 |
RMSD bond angle | 1.221 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.370 |
High resolution limit [Å] | 1.300 | 1.300 |
Rmerge | 0.080 | 0.500 |
Number of reflections | 88217 | |
<I/σ(I)> | 19.7 | 2.9 |
Completeness [%] | 99.7 | 100 |
Redundancy | 7.9 | 5.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 21.27% PEG 3350, 0.1M HEPES PH 6.5, MG-CHLORIDE 0.11M |