2JEE
Xray structure of E. coli YiiU
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-09-25 |
Detector | ADSC CCD |
Spacegroup name | P 1 |
Unit cell lengths | 40.386, 40.777, 80.134 |
Unit cell angles | 104.73, 97.03, 93.56 |
Refinement procedure
Resolution | 76.700 - 2.800 |
R-factor | 0.31 |
Rwork | 0.310 |
R-free | 0.32100 |
Structure solution method | MAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.020 |
RMSD bond angle | 1.770 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHELXD |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.950 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.060 | 0.360 |
Number of reflections | 11163 | |
<I/σ(I)> | 12.1 | 2.7 |
Completeness [%] | 95.5 | 95.5 |
Redundancy | 3.8 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |