2JD3
ParR from plasmid pB171
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-3 |
Synchrotron site | ESRF |
Beamline | ID14-3 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-09-01 |
Detector | ADSC CCD |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 96.768, 96.768, 124.945 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.000 - 2.800 |
R-factor | 0.2394 |
Rwork | 0.239 |
R-free | 0.27670 |
Structure solution method | MIR |
Starting model (for MR) | NONE |
RMSD bond length | 0.007 |
RMSD bond angle | 1.347 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SOLVE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.950 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.080 | 0.460 |
Number of reflections | 9015 | |
<I/σ(I)> | 23.3 | 5.3 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 11.6 | 12 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |