2J89

Functional and structural aspects of poplar cytosolic and plastidial type A methionine sulfoxide reductases

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE BM30A
Synchrotron site	ESRF
Beamline	BM30A
Temperature [K]	100
Spacegroup name	P 31
Unit cell lengths	68.561, 68.561, 40.678
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	25.000 - 1.700
R-factor	0.195
Rwork	0.195
R-free	0.20100
Structure solution method	OTHER
RMSD bond length	0.006
RMSD bond angle	1.310
Refinement software	CNS (1.1)

Data quality characteristics

	Overall
Low resolution limit [Å]	25.000
High resolution limit [Å]	1.700
Rmerge	0.050
Number of reflections	23121
<I/σ(I)>	8.6
Completeness [%]	98.2
Redundancy	10

Crystallization Conditions

crystal ID	method	pH	temperature	details
1