Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 113.2 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 77.315, 77.315, 74.162 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 54.640 - 2.300 |
| R-factor | 0.191 |
| Rwork | 0.188 |
| R-free | 0.25100 |
| Structure solution method | OTHER |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.635 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 2.300 |
| Rmerge | 0.120 |
| Number of reflections | 10441 |
| <I/σ(I)> | 7.8 |
| Completeness [%] | 99.9 |
| Redundancy | 4.87 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
