2J6K
N-TERMINAL SH3 DOMAIN OF CMS (CD2AP HUMAN HOMOLOG)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | ENRAF-NONIUS FR591 |
| Temperature [K] | 130 |
| Detector technology | CCD |
| Collection date | 2006-05-30 |
| Detector | MARRESEARCH |
| Spacegroup name | I 4 |
| Unit cell lengths | 120.018, 120.018, 153.930 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 94.490 - 2.770 |
| R-factor | 0.211 |
| Rwork | 0.208 |
| R-free | 0.27400 |
| Structure solution method | OTHER |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.465 |
| Data reduction software | MOSFLM |
| Data scaling software | TRUNCATE |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.300 | 2.790 |
| High resolution limit [Å] | 2.760 | 2.760 |
| Rmerge | 0.100 | 0.330 |
| Number of reflections | 27491 | |
| <I/σ(I)> | 10.98 | 0.95 |
| Completeness [%] | 97.2 | 81 |
| Redundancy | 3.47 | 3.26 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6.1 | 0.1 M SODIUM CITRATE PH 6.1, 25% PEG 4000, 20% ISOPROPANOL |
