2J69
Bacterial dynamin-like protein BDLP
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-4 |
| Synchrotron site | ESRF |
| Beamline | ID14-4 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC CCD |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 214.289, 218.596, 151.198 |
| Unit cell angles | 90.00, 134.81, 90.00 |
Refinement procedure
| Resolution | 50.000 - 3.000 |
| R-factor | 0.238 |
| Rwork | 0.236 |
| R-free | 0.28100 |
| Structure solution method | MAD |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.208 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 3.160 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Rmerge | 0.060 | 0.400 |
| Number of reflections | 86547 | |
| <I/σ(I)> | 11.5 | 2.1 |
| Completeness [%] | 98.6 | 98.5 |
| Redundancy | 1.9 | 1.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
