2J60
H-ficolin complexed to D-fucose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-11-17 |
Detector | ADSC CCD |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 62.000, 62.000, 346.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.000 - 1.800 |
R-factor | 0.214 |
Rwork | 0.212 |
R-free | 0.25800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2j3g |
RMSD bond length | 0.010 |
RMSD bond angle | 1.228 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 46.220 |
High resolution limit [Å] | 1.800 |
Rmerge | 0.120 |
Number of reflections | 29088 |
<I/σ(I)> | 12.5 |
Completeness [%] | 99.0 |
Redundancy | 6.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |