2J5Z

H-ficolin complexed to galactose

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-1
Synchrotron site	ESRF
Beamline	ID14-1
Temperature [K]	100
Detector technology	CCD
Collection date	2005-11-17
Detector	ADSC CCD
Spacegroup name	P 41 21 2
Unit cell lengths	62.200, 62.200, 345.490
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.000 - 1.730
R-factor	0.204
Rwork	0.202
R-free	0.23300
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2j3g
RMSD bond length	0.007
RMSD bond angle	1.047
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	AMoRE
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	46.220
High resolution limit [Å]	1.700
Rmerge	0.070
Number of reflections	74677
<I/σ(I)>	17.7
Completeness [%]	98.1
Redundancy	7.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1