2J5Y
Crystal structure of the GA module from F.magna
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-12-09 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 25.784, 58.068, 40.570 |
Unit cell angles | 90.00, 90.03, 90.00 |
Refinement procedure
Resolution | 40.560 - 1.400 |
R-factor | 0.151 |
Rwork | 0.148 |
R-free | 0.19900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1tf0 CHAIN B |
RMSD bond length | 0.015 |
RMSD bond angle | 1.610 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.480 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.070 | 0.240 |
Number of reflections | 22273 | |
<I/σ(I)> | 11.7 | 2.8 |
Completeness [%] | 94.4 | 72.6 |
Redundancy | 2.5 | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 22-26% (W/V) PEG 3350, 50 MM POTASSIUM PHOSPHATE PH 7.5, 100 MM AMMONIUM ACETATE |