2J3T
The crystal structure of the bet3-trs33-bet5-trs23 complex.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 4A |
| Synchrotron site | PAL/PLS |
| Beamline | 4A |
| Temperature [K] | 113 |
| Detector technology | CCD |
| Detector | ADSC CCD |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 57.602, 66.336, 200.808 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 30.000 - 2.400 |
| R-factor | 0.2074 |
| Rwork | 0.207 |
| R-free | 0.24870 |
| Structure solution method | SAD |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.262 |
| Data scaling software | HKL-2000 |
| Phasing software | SOLVE |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | |
| High resolution limit [Å] | 2.400 | 2.400 |
| Rmerge | 0.060 | |
| Number of reflections | 25464 | |
| <I/σ(I)> | 35.2 | 5.9 |
| Completeness [%] | 91.1 | 78.9 |
| Redundancy | 8.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8.5 | 20% (W/V) PEG 3350, 0.28 M LITHIUM SULFATE AND 0.1 M TRIS HCL (PH 8.5) |
