2J1R

Structure of a Streptococcus pneumoniae fucose binding module

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	113
Spacegroup name	P 21 21 21
Unit cell lengths	43.581, 60.390, 99.674
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	51.990 - 1.540
R-factor	0.156
Rwork	0.154
R-free	0.19800
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.018
RMSD bond angle	1.627
Phasing software	MOLREP
Refinement software	REFMAC (5.1.24)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	1.610
High resolution limit [Å]	1.550	1.550
Rmerge	0.060	0.360
Number of reflections	37211
<I/σ(I)>	14	3.3
Completeness [%]	99.8	99.7
Redundancy	4.6	3.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1