2J1P
Geranylgeranyl diphosphate synthase from Sinapis alba in complex with GGPP
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | MARRESEARCH |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 53.803, 91.551, 56.286 |
| Unit cell angles | 90.00, 96.89, 90.00 |
Refinement procedure
| Resolution | 32.000 - 1.800 |
| R-factor | 0.172 |
| Rwork | 0.170 |
| R-free | 0.20900 |
| Structure solution method | MAD |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.689 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 34.000 | 1.900 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Rmerge | 0.040 | 0.480 |
| Number of reflections | 94523 | |
| <I/σ(I)> | 10.6 | 1.6 |
| Completeness [%] | 95.6 | 91.5 |
| Redundancy | 2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
