2J1P

Geranylgeranyl diphosphate synthase from Sinapis alba in complex with GGPP

Experimental procedure

Experimental method	MAD
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	CCD
Detector	MARRESEARCH
Spacegroup name	P 1 21 1
Unit cell lengths	53.803, 91.551, 56.286
Unit cell angles	90.00, 96.89, 90.00

Refinement procedure

Resolution	32.000 - 1.800
R-factor	0.172
Rwork	0.170
R-free	0.20900
Structure solution method	MAD
RMSD bond length	0.019
RMSD bond angle	1.689
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	34.000	1.900
High resolution limit [Å]	1.800	1.800
Rmerge	0.040	0.480
Number of reflections	94523
<I/σ(I)>	10.6	1.6
Completeness [%]	95.6	91.5
Redundancy	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1