2J1G
L-ficolin complexed to N-acetyl-cystein
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-02-06 |
| Detector | ADSC CCD |
| Spacegroup name | P 32 |
| Unit cell lengths | 99.040, 99.040, 142.000 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 15.000 - 1.950 |
| R-factor | 0.178 |
| Rwork | 0.176 |
| R-free | 0.21000 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | PDP ENTRY 2J3G |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.091 |
| Phasing software | AMoRE |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 19.600 |
| High resolution limit [Å] | 1.950 |
| Rmerge | 0.070 |
| Number of reflections | 111804 |
| <I/σ(I)> | 15 |
| Completeness [%] | 98.5 |
| Redundancy | 6.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
