2J1D

Crystallization of hDaam1 C-terminal Fragment

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 24-ID-C
Synchrotron site	APS
Beamline	24-ID-C
Temperature [K]	100
Detector technology	CCD
Collection date	2006-02-12
Detector	ADSC CCD
Spacegroup name	I 2 2 2
Unit cell lengths	100.897, 100.343, 148.397
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.830 - 2.250
R-factor	0.22
Rwork	0.218
R-free	0.25000
Structure solution method	OTHER
RMSD bond length	0.009
RMSD bond angle	1.307
Data reduction software	XDS
Data scaling software	XDS
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	2.550
Rmerge	0.070
Number of reflections	24546
<I/σ(I)>	6.1
Completeness [%]	98.0
Redundancy	4.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		6.2		pH 6.20