2IXR
BipD of Burkholderia Pseudomallei
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-09-23 |
| Detector | ADSC CCD |
| Spacegroup name | C 2 2 2 |
| Unit cell lengths | 103.980, 122.790, 49.170 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 40.000 - 2.600 |
| R-factor | 0.2 |
| Rwork | 0.200 |
| Structure solution method | MIRAS |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.416 |
| Data scaling software | SCALA |
| Phasing software | SHELXD |
| Refinement software | TNT (5.6.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 38.100 | 2.740 |
| High resolution limit [Å] | 2.600 | 2.600 |
| Rmerge | 0.110 | 0.400 |
| Number of reflections | 10013 | |
| <I/σ(I)> | 18.7 | 5.4 |
| Completeness [%] | 99.7 | 98.6 |
| Redundancy | 10.9 | 9.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8.5 | 1 M TRISODIUM CITRATE, 10 MM SODIUM BORATE PH 8.5 |
