2INT

CRYSTAL STRUCTURE OF RECOMBINANT HUMAN INTERLEUKIN-4

Experimental procedure

Spacegroup name	P 41 21 2
Unit cell lengths	91.800, 91.800, 46.200
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 2.350
R-factor	0.232
Rwork	0.232
RMSD bond length	0.022
RMSD bond angle	2.400
Phasing software	X-PLOR
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	2.330 *
Rmerge	0.098 *
Total number of observations	86410 *
Number of reflections	8531 *
Completeness [%]	94.9 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	40 (mg/ml)
2	1	drop	ammonium sulfate	50 (%)
3	1	drop	sodium cacodylate	0.05 (M)
4	1	reservoir	ammonium sulfate	50 (%)
5	1	reservoir	sodium cacodylate	0.05 (M)