2IJL
The structure of a putative ModE from Agrobacterium tumefaciens.
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-ID |
| Synchrotron site | APS |
| Beamline | 19-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-11-02 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.97945, 0.97929 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 40.719, 79.536, 43.994 |
| Unit cell angles | 90.00, 106.70, 90.00 |
Refinement procedure
| Resolution | 39.770 - 2.300 |
| R-factor | 0.17665 |
| Rwork | 0.174 |
| R-free | 0.23623 |
| Structure solution method | MAD |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.480 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | HKL-3000 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 39.770 |
| High resolution limit [Å] | 2.300 |
| Number of reflections | 10719 |
| <I/σ(I)> | 12.3 |
| Completeness [%] | 94.0 |
| Redundancy | 3.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 0.2M LiSO4, 0.1M Bis-Tris ph 5.5, 25% PEG3350 , VAPOR DIFFUSION, HANGING DROP, temperature 293K |
