2II2
Crystal Structure of Alpha-11 Giardin
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-1 |
Synchrotron site | SSRL |
Beamline | BL9-1 |
Detector technology | CCD |
Collection date | 2006-07-04 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.979,0.905 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 45.951, 60.954, 119.909 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.740 - 1.100 |
R-factor | 0.196 |
Rwork | 0.195 |
R-free | 0.22500 |
Structure solution method | MAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.256 |
Data reduction software | HKL-2000 |
Data scaling software | d*TREK (9.2L) |
Phasing software | SOLVE (2.09) |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.740 | 1.140 |
High resolution limit [Å] | 1.100 | 1.100 |
Rmerge | 0.121 | 0.482 |
Total number of observations | 76436 | |
Number of reflections | 133460 | |
<I/σ(I)> | 6.4 | 2 |
Completeness [%] | 97.2 | 94.2 |
Redundancy | 9.01 | 5.98 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 277 | 200mM Lithium Sulfate, 100mM MES pH 6.0, 25% PEG 3350, VAPOR DIFFUSION, SITTING DROP, temperature 277K |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 277 | 200mM Lithium Sulfate, 100mM MES pH 6.0, 25% PEG 3350, VAPOR DIFFUSION, SITTING DROP, temperature 277K |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 277 | 200mM Lithium Sulfate, 100mM MES pH 6.0, 25% PEG 3350, VAPOR DIFFUSION, SITTING DROP, temperature 277K |