2IEW
Crystal structure of Inositol Phosphate Multikinase Ipk2 from S. cerevisiae
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X4A |
Synchrotron site | NSLS |
Beamline | X4A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-11-05 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.979 |
Spacegroup name | P 63 |
Unit cell lengths | 186.510, 186.510, 50.120 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.000 - 2.000 |
R-factor | 0.21123 |
Rwork | 0.208 |
R-free | 0.25293 |
Structure solution method | SAD |
RMSD bond length | 0.011 |
RMSD bond angle | 1.293 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.050 |
High resolution limit [Å] | 2.000 | 1.998 |
Rmerge | 0.067 | 0.392 |
Number of reflections | 58988 | |
<I/σ(I)> | 21.3 | 4 |
Redundancy | 4.7 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.7 | 293 | 100mM HEPES pH7.7, 200mM CaCl2, 28% PEG400, VAPOR DIFFUSION, SITTING DROP, temperature 293K |