2IA0
Transcriptional Regulatory Protein PF0864 From Pyrococcus Furiosus a Member of the ASNC Family (PF0864)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-06-17 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.97 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 58.074, 70.372, 96.536 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 56.890 - 2.370 |
R-factor | 0.2085 |
Rwork | 0.205 |
R-free | 0.26854 |
Structure solution method | AU SAD |
RMSD bond length | 0.014 |
RMSD bond angle | 1.793 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 56.890 | 2.420 |
High resolution limit [Å] | 2.370 | 2.370 |
Number of reflections | 14545 | |
<I/σ(I)> | 9 | 2.18 |
Completeness [%] | 91.7 | 50.29 |
Redundancy | 6.1 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MODIFIED MICROBATCH | 291 | MODIFIED MICROBACTH UNDER 0IL USING 1 MICROLITER DROPS CONTAING EQUAL VOLUMES OF PROTEIN 100 MM NAAC/HCL, 16% W/V PEG4000, PH4.5, TEMPERATURE 291K, MODIFIED MICROBATCH |