2I1X
Bacteriorhodopsin/lipid complex, D96A mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-1 |
Synchrotron site | SSRL |
Beamline | BL9-1 |
Temperature [K] | 100 |
Detector technology | CDD |
Collection date | 2005-04-14 |
Detector | ADSC QUANTUM |
Wavelength(s) | 0.97977 |
Spacegroup name | P 63 |
Unit cell lengths | 60.952, 60.952, 109.326 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 25.000 - 2.000 |
R-factor | 0.239 |
Rwork | 0.238 |
R-free | 0.29900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1c3w |
RMSD bond length | 0.015 |
RMSD bond angle | 0.054 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SHELX |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 2.090 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.062 | 0.756 |
Number of reflections | 15618 | |
<I/σ(I)> | 23.4 | 2.9 |
Completeness [%] | 100.0 | 99.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | CUBIC LIPID PHASE | 5.6 | 295 | MO:WATER:PHOSPHATE, pH 5.60, CUBIC LIPID PHASE, temperature 295K |