Experimental procedure
| Experimental method | MAD |
| Source type | ROTATING ANODE |
| Source details | BRUKER AXS MICROSTAR |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-09-15 |
| Detector | BRUKER PROTEUM X8 |
| Wavelength(s) | 1.54, 0.9798, 0.9795, 0.9568 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 29.070, 29.070, 184.710 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.000 - 1.470 |
| R-factor | 0.137 |
| Rwork | 0.139 |
| R-free | 0.22600 |
| Structure solution method | MAD |
| RMSD bond length | 0.007 |
| RMSD bond angle | 2.200 |
| Data reduction software | PROTEUM PLUS |
| Data scaling software | HKL-2000 |
| Phasing software | SOLVE |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 1.520 |
| High resolution limit [Å] | 1.470 | 1.470 |
| Number of reflections | 13454 | |
| Completeness [%] | 92.1 | 82.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 21% PEGmme550, 200mM Zn acetate, 0.1M MES pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
