2HYO
Crystal structure of Rv0805 N97A mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ELETTRA BEAMLINE 5.2R |
Synchrotron site | ELETTRA |
Beamline | 5.2R |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-01-19 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.2 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 55.215, 93.922, 51.136 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 51.160 - 2.250 |
R-factor | 0.315 |
Rwork | 0.210 |
R-free | 0.26800 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.241 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 51.160 | 2.306 |
High resolution limit [Å] | 2.250 | 2.250 |
Rmerge | 0.132 | 0.917 |
Number of reflections | 13212 | |
<I/σ(I)> | 9.5 | |
Completeness [%] | 99.8 | 99.9 |
Redundancy | 5.5 | 5.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 293 | MPD, MgCl2, MES, pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |