2HY1
Crystal structure of Rv0805
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ELETTRA BEAMLINE 5.2R |
Synchrotron site | ELETTRA |
Beamline | 5.2R |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-01-19 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.2 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 55.263, 94.299, 50.916 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.900 - 1.932 |
R-factor | 0.283 |
Rwork | 0.203 |
R-free | 0.22800 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.044 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.900 | 1.970 |
High resolution limit [Å] | 1.930 | 1.930 |
Rmerge | 0.065 | 0.375 |
Number of reflections | 20251 | |
<I/σ(I)> | 17.2 | |
Completeness [%] | 97.9 | 76.8 |
Redundancy | 4.9 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 293 | MPD, MgCl2, MES, pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |