2HFN
Crystal Structures of the Synechocystis Photoreceptor Slr1694 Reveal Distinct Structural States Related to Signaling
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 14-ID-B |
| Synchrotron site | APS |
| Beamline | 14-ID-B |
| Temperature [K] | 200 |
| Detector technology | CCD |
| Collection date | 2005-04-10 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 1.12714 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 90.927, 118.109, 97.100 |
| Unit cell angles | 90.00, 110.79, 90.00 |
Refinement procedure
| Resolution | 48.510 - 1.800 |
| R-factor | 0.24142 |
| Rwork | 0.240 |
| R-free | 0.26649 |
| Structure solution method | SAD |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.441 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.510 | 1.860 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Number of reflections | 163678 | |
| Completeness [%] | 97.3 | 99.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 0.1 M tri-sodium Citrate 20% PEG3350, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K |
