2H0L
Crystal Structure of a Mutant of Rat Annexin A5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ELLIOTT GX-21 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2004-04-04 |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 77.918, 78.959, 60.458 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.760 - 2.590 |
R-factor | 0.191 |
Rwork | 0.187 |
R-free | 0.27800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1a8a |
RMSD bond length | 0.011 |
RMSD bond angle | 1.263 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.760 | 2.740 |
High resolution limit [Å] | 2.590 | 2.590 |
Number of reflections | 10858 | |
<I/σ(I)> | 6.7 | 2.2 |
Completeness [%] | 95.7 | 96.6 |
Redundancy | 4 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | PEG 4000, 300MM SODIUM ACETATA, 100MM TRIS, 3MM SODIUM AZIDE, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 293K, pH 8.50 |