2GYD
Complex of equine apoferritin with the H-diaziflurane photolabeling reagent
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X6A |
Synchrotron site | NSLS |
Beamline | X6A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-11-08 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9791 |
Spacegroup name | F 4 3 2 |
Unit cell lengths | 181.890, 181.890, 181.890 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.130 - 1.720 |
R-factor | 0.208 |
Rwork | 0.207 |
R-free | 0.21700 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 1xz1 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.097 |
Data scaling software | d*TREK (9.4L) |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 37.130 | 37.130 | 1.780 |
High resolution limit [Å] | 1.720 | 3.710 | 1.720 |
Rmerge | 0.075 | 0.035 | 0.432 |
Total number of observations | 65154 | 28208 | |
Number of reflections | 27676 | ||
<I/σ(I)> | 16.9 | 40.4 | 2.8 |
Completeness [%] | 99.0 | 99.7 | 93 |
Redundancy | 18.94 | 21.02 | 10.12 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | 0.05 M cadmium sulfate, 0.1 M HEPES, and 1.0 M sodium acetate, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |