2GWO
crystal structure of TMDP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-18B |
| Synchrotron site | Photon Factory |
| Beamline | BL-18B |
| Temperature [K] | 93 |
| Detector technology | CCD |
| Collection date | 2002-11-08 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 1. |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 61.586, 72.240, 89.896 |
| Unit cell angles | 90.00, 99.66, 90.00 |
Refinement procedure
| Resolution | 40.000 - 2.400 |
| R-factor | 0.198 |
| Rwork | 0.198 |
| R-free | 0.25000 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.300 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | EPMR |
| Refinement software | CNS (0.9) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.000 | |
| High resolution limit [Å] | 2.400 | 2.400 |
| Number of reflections | 29452 | |
| Completeness [%] | 96.2 | 97.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 291 | 1.5M NaCl, 10% EtOH, 10mM DTT, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K |
