Loading
PDBj
MenuPDBj@FacebookPDBj@X(formerly Twitter)PDBj@BlueSkyPDBj@YouTubewwPDB FoundationwwPDBDonate
RCSB PDBPDBeBMRBAdv. SearchSearch help

2GRP

Crystal Structure of human RanGAP1-Ubc9-Y87A

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X4A
Synchrotron siteNSLS
BeamlineX4A
Temperature [K]100
Detector technologyCCD
Collection date2003-11-19
DetectorADSC QUANTUM 4
Wavelength(s)0.9797
Spacegroup nameP 1
Unit cell lengths39.429, 45.092, 60.871
Unit cell angles71.08, 71.11, 75.02
Refinement procedure
Resolution19.800 - 2.050
Rwork0.191
R-free0.23100
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.006
RMSD bond angle1.100
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareCNS (1.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0002.120
High resolution limit [Å]2.0502.050
Rmerge0.0500.166
Number of reflections22558
<I/σ(I)>16.8
Completeness [%]96.289.1
Redundancy21.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP5.52911M lithium sulfate, 0.5M ammonium sulfate, 50mM sodium citrate, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K

229380

PDB entries from 2024-12-25

PDB statisticsPDBj update infoContact PDBjnumon