2GQA
Structure of NADH-reduced SYE1, an OYE homologue from S. oneidensis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X13 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X13 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-05-02 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.8067 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 48.200, 83.739, 88.100 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.700 |
R-factor | 0.178 |
Rwork | 0.168 |
R-free | 0.19500 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.415 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.750 |
High resolution limit [Å] | 1.700 | 1.700 |
Number of reflections | 38791 | |
Completeness [%] | 99.9 | 99.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 1.8 amm. sulf, 2% PEF400, 0.1% bog, 0.1 M tris-hcl, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |