2GNQ
Structure of wdr5
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU FR-E |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2006-03-08 |
| Detector | RIGAKU RAXIS V |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 50.045, 55.323, 124.308 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 62.140 - 1.800 |
| R-factor | 0.151 |
| Rwork | 0.149 |
| R-free | 0.19200 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1vyh |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.277 |
| Data reduction software | CrystalClear ((MSC/RIGAKU)) |
| Data scaling software | HKL-2000 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 62.140 | 1.860 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Number of reflections | 30580 | |
| Completeness [%] | 93.0 | 62.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 300 | 20%peg5k mme, bis-tris 6.5, VAPOR DIFFUSION, SITTING DROP, temperature 300K |
