Experimental procedure
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-6A |
| Synchrotron site | Photon Factory |
| Beamline | BL-6A |
| Detector technology | DIFFRACTOMETER |
| Collection date | 1990-08-03 |
| Detector | WEISSENBERG |
| Wavelength(s) | 1.04 |
| Spacegroup name | P 62 2 2 |
| Unit cell lengths | 88.000, 88.000, 164.200 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 10.000 - 2.200 |
| R-factor | 0.202 |
| Rwork | 0.202 |
| R-free | 0.26000 |
| RMSD bond length | 0.014 |
| RMSD bond angle | 2.918 * |
| Data reduction software | WEIS |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 77.800 |
| High resolution limit [Å] | 2.200 |
| Rmerge | 0.053 * |
| Number of reflections | 24571 |
| Completeness [%] | 77.8 * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | Tris-HCl | 50 (mM) | |
| 2 | 1 | 1 | 5 (mM) | ||
| 3 | 1 | 1 | ammonium sulfate | 25 (%sat) |
