2GAE
Crystal structure of MltA from E. coli
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2004-04-29 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 103.880, 103.880, 110.560 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.000 - 2.500 |
R-factor | 0.256 |
Rwork | 0.253 |
R-free | 0.31000 |
Structure solution method | SAD |
RMSD bond length | 0.013 |
RMSD bond angle | 1.321 |
Data scaling software | d*TREK |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.077 | 0.445 |
Number of reflections | 23998 | |
<I/σ(I)> | 11.3 | 3.4 |
Completeness [%] | 97.6 | 93.7 |
Redundancy | 5.65 | 4.98 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.2 | 277 | 10 % PEG 8000, 100 mM sodium acetate, 10 mM magnesium chloride & 360 mM sodium chloride, pH 4.2, VAPOR DIFFUSION, HANGING DROP, temperature 277K |