2G62

Crystal structure of human PTPA

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	CCD
Collection date	2006-02-11
Detector	MARMOSAIC 225 mm CCD
Wavelength(s)	1.0
Spacegroup name	P 21 21 21
Unit cell lengths	48.190, 76.420, 87.300
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.900 - 1.600
R-factor	0.15361
Rwork	0.152
R-free	0.18339
Structure solution method	MAD
RMSD bond length	0.017
RMSD bond angle	1.587
Data reduction software	XDS
Data scaling software	XDS
Phasing software	SOLVE
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	1.700
High resolution limit [Å]	1.600	1.600
Rmerge	0.084	0.429
Number of reflections	43241
<I/σ(I)>	22.5	7.4
Completeness [%]	99.8	99.7
Redundancy	13.7	13.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1
1