2G4H
Anomalous substructure of apoferritin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X12 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X12 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-01-01 |
Detector | MARRESEARCH |
Wavelength(s) | 2.00 |
Spacegroup name | F 4 3 2 |
Unit cell lengths | 182.160, 182.160, 182.160 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.000 |
R-factor | 0.19594 |
Rwork | 0.195 |
R-free | 0.21772 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.017 |
RMSD bond angle | 1.511 |
Data reduction software | HKL-2000 |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | FFT |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 2.000 |
Number of reflections | 18033 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |