2FKE

FK-506-BINDING PROTEIN: THREE-DIMENSIONAL STRUCTURE OF THE COMPLEX WITH THE ANTAGONIST L-685,818

Experimental procedure

Spacegroup name	P 42 21 2
Unit cell lengths	58.154, 58.154, 55.445
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 1.720
R-factor	0.18
RMSD bond length	0.018
RMSD bond angle	0.035
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	1.720 *
Rmerge	0.059 *
Total number of observations	64522 *
Number of reflections	11113 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	5.1 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir		47 (%sat)
2	1	reservoir	potassium formate	0.1 (M)
3	1	reservoir		0.02 (%)