2FBN

Plasmodium falciparum putative FK506-binding protein PFL2275c, C-terminal TPR-containing domain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU FR-E
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2005-12-05
Detector	RIGAKU RAXIS IV
Spacegroup name	P 21 21 21
Unit cell lengths	56.239, 62.936, 103.334
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.000 - 1.630
R-factor	0.2008
Rwork	0.200
R-free	0.23522
Structure solution method	SAD
RMSD bond length	0.011
RMSD bond angle	1.114
Data reduction software	CrystalClear ((MSC/RIGAKU))
Data scaling software	HKL-2000
Phasing software	SOLVE
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.660
High resolution limit [Å]	1.630	1.630
Rmerge	0.043	0.507
Number of reflections	41003
<I/σ(I)>	19.4	1.64
Completeness [%]	88.0	31
Redundancy	6	2.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION	4.6	296	3.5 M NaFormate, 0.1 M NaAcetate pH 4.6, VAPOR DIFFUSION, temperature 296K
1	VAPOR DIFFUSION	4.6	296	3.5 M NaFormate, 0.1 M NaAcetate pH 4.6, VAPOR DIFFUSION, temperature 296K