2FA4
Crystal Structure of Oxidized Form from Saccharomyces cerevisiae
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2005-08-30 |
Detector | MARRESEARCH |
Wavelength(s) | 1.54179 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 83.151, 83.151, 64.732 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.160 - 2.380 |
R-factor | 0.20818 |
Rwork | 0.206 |
R-free | 0.25861 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.022 |
RMSD bond angle | 1.591 |
Data reduction software | MOSFLM |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.165 | |
High resolution limit [Å] | 2.376 | 2.400 |
Number of reflections | 9445 | |
Completeness [%] | 98.3 | 98 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 4.6 | 289 | 0.2M ammonium sulfate, 0.1M sodium acetate buffer, 30%(w/v) PEG mmE 2000, pH 4.6, EVAPORATION, temperature 289K |