2ES7
Crystal structure of Q8ZP25 from Salmonella typhimurium LT2. NESG TARGET STR70
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X4A |
| Synchrotron site | NSLS |
| Beamline | X4A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-08-01 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.97925, 0.97955, 0.96782 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 39.549, 71.156, 95.004 |
| Unit cell angles | 90.00, 90.11, 90.00 |
Refinement procedure
| Resolution | 19.900 - 2.800 |
| R-factor | 0.285 |
| Rwork | 0.285 |
| R-free | 0.33800 |
| Structure solution method | MAD |
| RMSD bond length | 0.017 |
| RMSD bond angle | 2.400 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.850 |
| High resolution limit [Å] | 2.800 | 2.800 |
| Rmerge | 0.049 | 0.122 |
| Number of reflections | 25130 | |
| <I/σ(I)> | 35.37 | 9.5 |
| Completeness [%] | 98.9 | 97.4 |
| Redundancy | 4 | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | VAPOR DIFFUSION, HANGING DROP |
