Experimental procedure
Spacegroup name | P 1 21 1 |
Unit cell lengths | 42.110, 51.680, 45.060 |
Unit cell angles | 90.00, 109.37, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.500 |
R-factor | 0.105 |
R-free | 0.15400 |
RMSD bond length | 0.012 |
RMSD bond angle | 0.031 |
Refinement software | SHELXL |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.480 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | enzyme | 10 (mg/ml) | |
2 | 1 | reservoir | Tris-HCl | 20 (mM) | pH8.0 |
3 | 1 | reservoir | PEG8000 | 10-22 (%(w/v)) |